A low temperature reduction of CCl4 to solid and hollow carbon nanospheres using metallic sodium.

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dc.contributor.authorChoucair, Men_AU
dc.contributor.authorHill, MRen_AU
dc.contributor.authorStride, JAen_AU
dc.date.accessioned2018-09-14T00:52:56Zen_AU
dc.date.available2018-09-14T00:52:56Zen_AU
dc.date.issued2015-03-15en_AU
dc.date.statistics2017-08-22en_AU
dc.description.abstractCarbon nanospheres are obtained by reacting metallic sodium at 100 °C with tetrachloromethane under a flow of N2 gas at ambient pressure. The product consisted of both hollowed and solid carbon spheres, ranging between 20 and 300 nm in size and comprised of concentrically oriented, disordered graphitic fragments. The maximum surface area recorded for this nanostructured carbon is 830 m2 g−1. Morphological, structural, and chemical analysis of the product is carried out with HR-TEM, BET surface area, XPS, XRD, and Raman spectroscopy. The formation of the spherical shape of the carbon nanoparticles is discussed based on direct observations of the reaction at the interfacial phase boundary.Copyright © 2017 Elsevier B.V.en_AU
dc.identifier.citationChoucair, M., Hill, M. R., & Stride, J. A. (2015). A low temperature reduction of CCl4 to solid and hollow carbon nanospheres using metallic sodium. Materials Chemistry and Physics, 154, 38-43. doi:10.1016/j.matchemphys.2015.01.042en_AU
dc.identifier.govdoc8752en_AU
dc.identifier.issn0254-0584en_AU
dc.identifier.journaltitleMaterials Chemistry and Physicsen_AU
dc.identifier.pagination38-43en_AU
dc.identifier.urihttp://dx.doi.org/10.1016/j.matchemphys.2015.01.042en_AU
dc.identifier.urihttp://apo.ansto.gov.au/dspace/handle/10238/8978en_AU
dc.identifier.volume154en_AU
dc.language.isoenen_AU
dc.publisherElsevieren_AU
dc.subjectNanostructuresen_AU
dc.subjectInterfacesen_AU
dc.subjectFullerenesen_AU
dc.subjectElectron microscopyen_AU
dc.subjectSodiumen_AU
dc.subjectCarbonen_AU
dc.titleA low temperature reduction of CCl4 to solid and hollow carbon nanospheres using metallic sodium.en_AU
dc.typeJournal Articleen_AU
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