Diffraction study on the thermal stability of Ti3SiC2/TiC/TiSi2 composites in vacuum

dc.contributor.authorPang, WKen_AU
dc.contributor.authorLow, IMen_AU
dc.contributor.authorO’Connor, BHen_AU
dc.contributor.authorStuder, AJen_AU
dc.contributor.authorPeterson, VKen_AU
dc.contributor.authorPalmquist, JPen_AU
dc.date.accessioned2012-04-18T01:11:07Zen_AU
dc.date.available2012-04-18T01:11:07Zen_AU
dc.date.issued2009-06-29en_AU
dc.date.statistics2012-04-18en_AU
dc.description.abstractTitanium silicon carbide (Ti3SiC2) possesses a unique combination of properties of both metals and ceramics, for it is thermally shock resistant, thermally and electrically conductive, damage tolerant, lightweight, highly oxidation resistant, elastically stiff, and mechanically machinable. In this paper, the effect of high vacuum annealing on the phase stability and phase transitions of Ti3SiC2/TiC/TiSi2 composites at up to 1550° C was studied using in‐situ neutron diffraction. The role of TiC and TiSi2 on the thermal stability of Ti3SiC2 during vacuum annealing is discussed. TiC reacts with TiSi2 between 1400–1450°C to form Ti3SiC2. Above 1400° C, decomposition of Ti3SiC2 into TiC commenced and the rate increased with increased temperature and dwell time. Furthermore, the activation energy for the formation and decomposition of Ti3SiC2 was determined. © 2009 American Institute of Physicsen_AU
dc.identifier.citationPang, W. K., Low I. M., O'Connor, B. H., Studer, A. J., Peterson, V. K., Palmquist, J. P. (2009). Diffraction study on the thermal stability of Ti3SiC2/TiC/TiSi2 composites in vacuum. Paper presented to the International Conference on Neutron and X‐Ray Scattering—2009, 29th June-1st July 2009, Kuala Lumpur, Malaysia. In "Neutron and X‐ray Scattering in Advancing Materials Research." Proceedings of the International Conference on Neutron and X‐Ray Scattering—2009, A. A. B. Mohamed (Eds). AIP Conference Proceedings, 1202(1), 44-48. doi:10.1063/1.3295608en_AU
dc.identifier.conferenceenddate1 July 2009en_AU
dc.identifier.conferencenameInternational Conference on Neutron and X‐Ray Scattering—2009en_AU
dc.identifier.conferenceplaceKuala Lumpur, Malaysiaen_AU
dc.identifier.conferencestartdate29 June 2009en_AU
dc.identifier.govdoc4294en_AU
dc.identifier.isbn978-0-7354-0739-8en_AU
dc.identifier.isbn9780735407398en_AU
dc.identifier.issn0094-243Xen_AU
dc.identifier.issue1en_AU
dc.identifier.journaltitleAIP Conference Proceedingsen_AU
dc.identifier.pagination44-48en_AU
dc.identifier.placeofpublicationA. A. B. Mohameden_AU
dc.identifier.urihttp://dx.doi.org/10.1063/1.3295608en_AU
dc.identifier.urihttp://apo.ansto.gov.au/dspace/handle/10238/4146en_AU
dc.identifier.volume1202en_AU
dc.language.isoenen_AU
dc.publisherAmerican Institute of Physicsen_AU
dc.subjectDiffractionen_AU
dc.subjectTemperature surveysen_AU
dc.subjectNeutron diffractionen_AU
dc.subjectPhase transformationsen_AU
dc.subjectTemperature range 1000-4000 Ken_AU
dc.subjectDecompositionen_AU
dc.titleDiffraction study on the thermal stability of Ti3SiC2/TiC/TiSi2 composites in vacuumen_AU
dc.typeConference Paperen_AU
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