An in situ rapid heat-quench cell for small-angle neutron scattering

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dc.contributor.authorPullen, SAen_AU
dc.contributor.authorGilbert, EPen_AU
dc.contributor.authorOlsen, SRen_AU
dc.contributor.authorLang, EAen_AU
dc.contributor.authorDoolan, KRen_AU
dc.date.accessioned2009-10-06T04:03:18Zen_AU
dc.date.accessioned2010-04-30T05:06:48Zen_AU
dc.date.available2009-10-06T04:03:18Zen_AU
dc.date.available2010-04-30T05:06:48Zen_AU
dc.date.issued2008-06en_AU
dc.date.statistics2008-06en_AU
dc.description.abstractA dual-temperature sample environment has been developed enabling the rapid heating and quenching of samples in situ for small-angle neutron scattering (SANS). The rapid heat and quench cell (RHQC) allows samples to be rapidly heated up to 600 K and then quenched to 150 K, or vice versa, in a single shot or cycle mode, with the sample in position for data collection. Measured cooling rates of up to 11 K s-1 and heating rates up to 19 K s-1 have been recorded during the testing stages. First results using the RHQC on a hydrogenated/deuterated paraffin blend quenched from the melt illustrate the value of the device in accessing the early stage phase separation kinetics with SANS. © 2008, Institute of Physicsen_AU
dc.identifier.articlenumber065707en_AU
dc.identifier.citationPullen, S. A., Gilbert, E. P., Olsen, S. R., Lang, E. A., & Doolan, K. R. (2008). An in situ rapid heat-quench cell for small-angle neutron scattering. Measurement Science and Technology, 19(6), 065707. doi:0.1088/0957-0233/19/6/065707en_AU
dc.identifier.govdoc1435en_AU
dc.identifier.issn0957-0233en_AU
dc.identifier.issue6en_AU
dc.identifier.journaltitleMeasurement Science and Technologyen_AU
dc.identifier.urihttp://dx.doi.org/10.1088/0957-0233/19/6/065707en_AU
dc.identifier.urihttp://apo.ansto.gov.au/dspace/handle/10238/1931en_AU
dc.identifier.volume19en_AU
dc.language.isoenen_AU
dc.publisherInstitute of Physicsen_AU
dc.subjectSmall angle scatteringen_AU
dc.subjectQuenchingen_AU
dc.subjectHeatingen_AU
dc.subjectIn-situ processingen_AU
dc.subjectSample preparationen_AU
dc.subjectSeparation processesen_AU
dc.titleAn in situ rapid heat-quench cell for small-angle neutron scatteringen_AU
dc.typeJournal Articleen_AU
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