Electrochemical cell for neutron reflectometry studies of the structure of ionic liquids at electrified interface

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dc.contributor.authorLauw, Yen_AU
dc.contributor.authorRodopoulos, Ten_AU
dc.contributor.authorGross, Men_AU
dc.contributor.authorNelson, Aen_AU
dc.contributor.authorGardner, Ren_AU
dc.contributor.authorHorne, MDen_AU
dc.date.accessioned2010-09-01T05:12:50Zen_AU
dc.date.available2010-09-01T05:12:50Zen_AU
dc.date.issued2010-07en_AU
dc.date.statistics2010-07en_AU
dc.description.abstractWe describe the design and use of a closed three-electrode electrochemical cell for neutron reflectometry studies of the structure of the electrical double-layer in ionic liquids. A transparent glass counter electrode was incorporated to allow easy monitoring of any gas bubbles trapped in the cell. A 100 mm diameter silicon wafer polished to 0.1 nm rms roughness coated with gold over a chromium adhesion layer was used as the working electrode. The utility of the cell was demonstrated during neutron reflectometry measurements of the ultrahigh purity ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide ([C4mpyr][NTf2]) at two different applied potentials. © 2010, American Institute of Physicsen_AU
dc.identifier.articlenumber74101en_AU
dc.identifier.citationLauw, Y., Rodopoulos, T., Gross, M., Nelson, A., Gardner, R., & Home, M. D. (2010). Electrochemical cell for neutron reflectometry studies of the structure of ionic liquids at electrified interface. Review of Scientific Instruments, 81(7), 074101. doi:10.1063/1.3455178en_AU
dc.identifier.govdoc2561en_AU
dc.identifier.issn0034-6748en_AU
dc.identifier.issue7en_AU
dc.identifier.journaltitleReview of Scientific Instrumentsen_AU
dc.identifier.urihttp://dx.doi.org/10.1063/1.3455178en_AU
dc.identifier.urihttp://apo.ansto.gov.au/dspace/handle/10238/2404en_AU
dc.identifier.volume81en_AU
dc.language.isoenen_AU
dc.publisherAmerican Institute of Physicsen_AU
dc.subjectElectrochemical cellsen_AU
dc.subjectElectrodesen_AU
dc.subjectSiliconen_AU
dc.subjectNeutron reflectorsen_AU
dc.subjectLiquidsen_AU
dc.subjectLayersen_AU
dc.titleElectrochemical cell for neutron reflectometry studies of the structure of ionic liquids at electrified interfaceen_AU
dc.typeJournal Articleen_AU
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