Lead-210: a contaminant in particle detectors for dark matter studies

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Date
2021-11-17
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Australian Nuclear Science and Technology Organisation
Abstract
The DAMA/LIBRA (DArk Matter/Large sodium Iodide Block for RAre processes) is a very low background NaI(Tl) detector array that has been running for two decades in the Gran Sasso underground laboratory in Italy. It gives a robust annual modulation signal in the 2 to 6 keV region that may be due to dark matter [1]. In order to verify this result with higher sensitivity, the SABRE (Sodium iodide with Active Background REjection) experiment [2] is being developed. Radioimpurities such as ⁴ ⁰ K, ²³⁸ U, ²¹⁰ Pb and ²³²Th, either intrinsic to the detector material or surface contamination, provide a fundamental limit to the sensitivity of SABRE. Therefore, it is crucial to characterise this background for improved identification of any additional signal above it. Here, we focus on ²¹⁰ Pb (half-life of 22.2 years) as its beta decay to ²¹⁰ Bi contributes to the low-energy “dark matter” spectra [3]. Lead-210 measurements are usually performed using alpha -, beta - or gamma counting depending on the sample size and concentration [4]. However, in recent years, the interest and therefore developments to measure ²¹⁰ Pb using accelerator mass spectrometry (AMS) has increased [5], [6]. From a chemical point of view, we need to optimise the Pb extraction of ~1 mg of stable Pb carrier through precipitations and ion exchange chromatography using about a kilogram of NaI. This is not trivial and methods using two different resins, i.e., 1x8 anion exchange resin and Sr® resin, have been tested. It is also essential that the stable Pb carrier and any material and chemical product in use should contain as little ²¹⁰ Pb as possible. Hence, several materials have been investigated including a piece from a 16th century roof and radiation shielding blocks as a source of Pb carrier. Furthermore, we studied PbO and PbF₂ samples to identify the optimal negative-ion beam and the suitability of using either Fe₂ O₃ or NaF as bulk material for the AMS target to reduce the stable Pb content. AMS measurements related to this work have been made using the 14UD pelletron accelerator at the Australian National University and the 1 MV VEGA accelerator at the Australian Nuclear Science and Technology Organisation.
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Keywords
Lead 210, Nonluminous matter, Particles, Detection, Laboratories, Italy, keV range 01-10, Sodium iodides, Reflection, Mass spectroscopy, ANSTO
Citation
Froehlich, M., Merchel, S., Slavkovská, Z., Dastgir, F., Fifield, L. K., Hotchkis, M., Koll. D., Pavetich, S., Tims, S., & Wallner, A. (2021). Lead-210: a contaminant in particle detectors for dark matter studies. Paper presented to the 15th International Conference on Accelerator Mass Spectrometry. ANSTO Sydney, Australia. November 15th – 19th, 2021. (pp. 254). Retrieved from: https://ams15sydney.com/wp-content/uploads/2021/11/AMS-15-Full-Program-and-Abstract-Book-R-1.pdf