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Please use this identifier to cite or link to this item: http://apo.ansto.gov.au/dspace/handle/10238/8128

Title: Microstructure and texture analysis of [delta]-hydride precipitation in Zircaloy-4 materials by electron microscopy and neutron diffraction
Authors: Wang, Z
Garbe, U
Li, H
Wang, Y
Studer, AJ
Sun, G
Harrison, RP
Liao, X
Vicente Alvarez, MA
Santisteban, JR
Kong, C
Keywords: MICROSTRUCTURE
ZIRCALOY
NEUTRON DIFFRACTION
MICROSCOPY
ELECTRON SOURCES
ZIRCONIUM ALLOYS
Issue Date: 1-Jan-2014
Publisher: IUCR
Citation: Wang, Z., Garbe, U., Li, H., Wang, Y., Studer, A. J., Sun, G., . . . Kong, C. (2014). Microstructure and texture analysis of [delta]-hydride precipitation in Zircaloy-4 materials by electron microscopy and neutron diffraction. Journal of Applied Crystallography, 47(1), 303-315. doi: doi: http://dx.doi.org/10.1107/S1600576713031956
Abstract: This work presents a detailed microstructure and texture study of various hydrided Zircaloy-4 materials by neutron diffraction and microscopy. The results show that the precipitated [delta]-ZrH1.66 generally follows the [delta](111)//[alpha](0001) and [delta][1{\overline 1}0]//[alpha][11{\overline 2}0] orientation relationship with the [alpha]-Zr matrix. The [delta]-hydride displays a weak texture that is determined by the texture of the [alpha]-Zr matrix, and this dependence essentially originates from the observed orientation correlation between [alpha]-Zr and [delta]-hydride. Neutron diffraction line profile analysis and high-resolution transmission electron microscopy observations reveal a significant number of dislocations present in the [delta]-hydride, with an estimated average density one order of magnitude higher than that in the [alpha]-Zr matrix, which contributes to the accommodation of the substantial misfit strains associated with hydride precipitation in the [alpha]-Zr matrix. The present observations provide an insight into the behaviour of [delta]-hydride precipitation in zirconium alloys and may help with understanding the induced embrittling effect of hydrides.© 2014, International Union of Crystallography.
URI: http://dx.doi.org/10.1107/S1600576713031956
http://apo.ansto.gov.au/dspace/handle/10238/8128
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