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|Title: ||In situ synchrotron high-energy x-ray diffraction analysis on phase transformations in Ti-Al alloys processed by equal-channel angular pressing.|
|Authors: ||Liss, KD|
|Keywords: ||Phase Transformations|
High Energy Physics
|Issue Date: ||Nov-2009|
|Citation: ||Liss, K. D., Whitfield, R. E., Xu, W., Buslaps, T., Yeoh, L. A., & Wu, X. L., et al. (2009). In situ synchrotron high-energy x-ray diffraction analysis on phase transformations in Ti-Al alloys processed by equal-channel angular pressing. Journal of Synchrotron Radiation, 16, 825-834.|
|Abstract: ||Mixtures of 47-Al and 53-Ti powders (atomic %) have been consolidated using back pressure equal-channel angular pressing starting with both raw and ball-milled powders. In situ synchrotron high-energy X-ray diffraction studies are presented with continuous Rietveld analysis obtained upon a heating ramp from 300 K to 1075 K performed after the consolidation process. Initial phase distributions contain all intermetallic compounds of this system except Al, with distribution maxima in the outer regions of the concentrations (α-Ti, TiAl3). Upon annealing, the phase evolution and lattice parameter changes owing to chemical segregation, which is in favour for the more equilibrated phases such as γ-TiAl, α(2)-Ti3Al and TiAl2, were followed unprecedentedly in detail. An initial δ-TiH2 content with a phase transition at about 625 K upon heating created an intermediate β-Ti phase which played an important role in the reaction chain and gradually transformed into the final products. © 2009, Wiley-Blackwell. The definitive version is available at www3.interscience.wiley.com|
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