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Browsing by Author "van Wyngaardt, WM"

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Accuracy of dose calibrators for 68Ga PET imaging: unexpected findings in a multicenter clinical pretrial assessment
(Society of Nuclear Medicine and Molecular Imaging (SNMMI), 2018-04) Bailey, DL; Hofman, MS; Forwood, NJ; O'Keefe, GJ; Scott, AM; van Wyngaardt, WM; Howe, B; Kovacev, O; Francis, RJ; ARTnet; ProPMSA Trial Investigators
We report the discovery of a systematic miscalibration during the work-up process for site validation of a multicenter clinical PET imaging trial using 68Ga, which manifested as a consistent and reproducible underestimation in the quantitative accuracy (assessed by SUV) of a range of PET systems from different manufacturers at several different facilities around Australia. Methods: Sites were asked to follow a strict preparation protocol to create a radioactive phantom with 68Ga to be imaged using a standard clinical protocol before commencing imaging in the trial. All sites had routinely used 68Ga for clinical PET imaging for many years. The reconstructed image data were transferred to an imaging core laboratory for analysis, along with information about ancillary equipment such as the radionuclide dose calibrator. Fourteen PET systems were assessed from 10 nuclear medicine facilities in Australia, with the aim for each PET system being to produce images within 5% of the true SUV. Results: At initial testing, 10 of the 14 PET systems underestimated the SUV by 15% on average (range, 13%–23%). Multiple PET systems at one site, from two different manufacturers, were all similarly affected, suggesting a common cause. We eventually identified an incorrect factory-shipped dose calibrator setting from a single manufacturer as being the cause. The calibrator setting for 68Ga was subsequently adjusted by the users so that the reconstructed images produced accurate values. Conclusion: PET imaging involves a chain of measurements and calibrations to produce accurate quantitative performance. Testing of the entire chain is simple, however, and should form part of any quality assurance program or prequalifying site assessment before commencing a quantitative imaging trial or clinical imaging. © 2018 by the Society of Nuclear Medicine and Molecular Imaging
APMP comparison of the activity measurements of Ba-133 (APMP.RI(II)-K2.Ba-133) and links to the SIR
(Institute of Physics, 2009-01-01) Yunoki, A; Mo, L; Shaha, VV; Kartubi, N; van Wyngaardt, WM; Yuan, MC; Nhan, DD; Park, TS; Yuandi, Y; Soodprasert, T; Michotte, C
The international comparison of radioactivity measurements of 133Ba (APMP.RI(II)-K2.Ba-133) was carried out within the framework of the Asia-Pacific Metrology Programme (APMP). In total, ten institutes took part in the comparison, and five institutes undertook absolute measurements. Nine of the results agreed with each other within their specified uncertainties. The source from the same radioactive solution that was used in the comparison was sent to the BIPM/SIR in order to link this regional comparison to the BIPM key comparison reference value (KCRV). The degrees of equivalence between the APMP comparison and the other measurements for 133Ba are presented. © 2009, Institute of Physics
Capability development for the quantification of Ba-133 in milk powder by gamma-ray spectrometry
(South Pacific Environmental Radioactivity Association, 2018-11-06) Van De Voorde, R; Mokhber-Shahin, L; Harrison, JJ; van Wyngaardt, WM; Jackson, TW
Barium-133 (Ba-133) is a fission product with a half-life of 10.5 years. It decays to its daughter radionuclide Cs-183 by electron capture, emitting multiple characteristic gamma emissions. The capability to accurately quantify Ba-133 is of importance due to its persistence in the environment. This is enabled by its relatively long half-life and its uptake into the food chain due to its similarity in chemical properties to calcium. Therefore, screening for contamination of calcium-rich foodstuffs such as milk and milk powders, is required following a nuclear or radioactive contamination event. Refining a capability to quantify Ba-138 utilising gamma-ray spectrometry is advantageous due to its requirement of minimal sample preparation and usefulness in screening for a wide range of other radionuclides, therefore providing critical information in a relatively timely manner. in the 2017 IAEA ALMERA proficiency test exercise ANSTO’s Radioanalytical Chemistry Capability group demonstrated its proficiency in quantifying Ba-138 in water, and in quantifying other nuclides such as Cs-187 and Sr-90 in milk powder. However, the activity concentration of Ba-188 in the milk powder matrix was lower than the target value. Therefore, a study was undertaken to optimise a method for accurately quantifying Ba-138 in milk powder by gamma-ray spectrometry, holistically investigating the entire process from sample receipt and storage to counting geometry and interpretation of data. A series of storage and drying experiments were undertaken to optimise a method for determining the moisture content of a variety of supermarket bought milk powders, comparing measured mass changes using both desiccator and benchtop cooling following oven-drying. The impact of storage following unsealing the received sample container on moisture content was investigated and its implications on subsequent internal and cross-laboratory analysis were explored. The milk powders were packed into various geometries and analysed by gamma-ray spectrometry to quantify the naturally-occurring radionuclides present in the milk powder. This data was used to better understand the matrix and investigate the possible interference of naturally-occurring radionuclides in the quantification of Ba-188. Milk powders were also purposefully spiked with known activities of Ba-133 and a comparison of various counting geometries, the impact of sample density and self-absorption on counting efficiency were investigated. The use of a variety of calibration standards of varying geometries and densities was also explored to assess their applicability to the milk powder matrix. This paper will detail the investigation findings and propose recommendations for a more reliable method for the quantification of Ba-133 in milk powder by gamma-ray spectrometry to be hence employed in ANSTO’s Radioanalytical Chemistry Capability laboratory.
Characterisation of a well-type NaI(T1) detector by means of a Monte Carlo simulation for radionuclide metrology application
(Elsevier B. V., 2021-10) Heranudin, H; Smith, ML; van Wyngaardt, WM; Guatelli, S; Li, E; Rosenfeld, AB
A well-type NaI(Tl) detector was modelled and characterised by means of a Monte Carlo simulation, as part of a project to develop a 4πβ (Plastic Scintillator)-4πγ instrument to be used for the primary standardisation of radionuclides at ANSTO. The simulation based on GEANT4 was used to characterise the 4πγ detector in terms of potential dead layer/inactive materials, full energy peak efficiency, coincidence-summing correction, and energy resolution. An excellent agreement was obtained between the simulation results and the experimental measurements. © 2021 Elsevier Ltd.
Comparison of triple-to-double coincidence ratio (TDCR) efficiency calculations and uncertainty assessments for Tc-99
(Elsevier, 2010-07) Zimmerman, BE; Altzitzoglou, T; Rodrigues, D; Broda, R; Cassette, P; Mo, L; Ratel, G; Simpson, BRS; van Wyngaardt, WM; Watjen, C
A comparison exercise for data analysis was recently conducted by the Liquid Scintillation Counting Working Group (LSCWG) of the International Committee on Radionuclide Metrology (ICRM) to evaluate the uncertainties involved in applying different analysis methodologies (including computer programs) for the triple-to-double coincidence ratio (TDCR) method. The goals of the comparison were to (1) study differences in calculation results from different TDCR analysis programs, (2) investigate differences in analysis techniques and uncertainty assessment philosophies between laboratories, and (3) study the effect of not taking asymmetry of photomultiplier tube (PMT) efficiencies into account on the calculated activity. To achieve this, a single set of TDCR data for the pure beta emitter 99Tc, was distributed to the participants, who analyzed the data according to their normal procedures and report the activity concentration of the 99Tc solution from their results. The results indicate that the presently used programs are generally able to calculate the same activity values, assuming that the correct input parameters are used and that not taking PMT asymmetry into account in the calculations can lead to significant (0.6% for 99Tc) errors in reported results. The comparison also highlighted the need for a more rigorous approach to estimating and reporting uncertainties. © 2010, Elsevier Ltd.
Development of activity standard for 90Y microspheres
(Elsevier, 2005-08) Mo, L; Avci, B; James, D; Simpson, BRS; van Wyngaardt, WM; Cessna, JT; Baldock, C
90Y microspheres are important therapeutic radiopharmaceuticals used in the treatment of liver cancer through a process known as selective internal radiation therapy. SIR-spheres® is a radiopharmaceutical product that is comprised of 90Y microspheres suspended in sterile, pyrogen-free water for injection into patients. It is necessary to establish for the SIR-spheres® production the capability of accurately measuring the activity of this product to a traceable national measurement standard. An activity standard for SIR-spheres® was developed from a standard for 90Y solution, employing a highly quantifiable chemical digestion process. Calibration factors for the manufacturer's ionisation chambers were determined for 1 and 5 ml of the SIR-spheres® product placed in Wheaton vials, for both 34% and 44% of 90Y microsphere concentration. © 2005, Elsevier Ltd.
Development of the Australian standard for germanium-68 by two liquid scintillation counting methods
(Elsevier B. V., 2018-04) van Wyngaardt, WM; Smith, ML; Jackson, TW; Howe, B; Tobin, SM; Reinhard, MI
In response to the increasing application of 68Ge/68Ga and 68Ga in nuclear medicine, an international comparison of activity measurement of 68Ge in equilibrium with 68Ga was organised. ANSTO standardised the comparison solution by the 4π(LS)β+-γ coincidence extrapolation and TDCR efficiency calculation methods, with excellent agreement between the two results. The primary standard was transferred to the ANSTO Secondary Standard Ionisation Chamber. Internationally traceable Australian Certified Reference Materials (ACRMs) of 68Ge/68Ga can now be prepared in various measurement geometries applied in nuclear medicine. © 2017 Crown Copyright, Published by Elsevier Ltd. All
Evidence against solar influence on nuclear decay constants
(Elsevier B. V., 2016-10-10) Pommé, S; Stroh, H; Paepen, J; Van Ammel, R; Marouli, M; Altzitzoglou, T; Hult, M; Kossert, K; Nähle, O; Schrader, H; Juget, F; Bailat, CJ; Nedjadi, Y; Bochud, F; Buchillier, T; Michotte, C; Courte, S; van Rooy, MW; van Staden, MJ; Lubbe, J; Simpson, BRS; Fazio, A; De Felice, P; Jackson, TW; van Wyngaardt, WM; Reinhard, MI; Golya, J; Bourke, S; Roy, T; Galea, R; Keightley, JD; Ferreira, KM; Collins, SM; Ceccatelli, A; Unterweger, MP; Fitzgerald, R; Bergeron, DE; Pibida, L; Verheyen, L; Bruggeman, M; Vodenik, B; Korun, M; Chisté, V; Amiot, MN
The hypothesis that proximity to the Sun causes variation of decay constants at permille level has been tested and disproved. Repeated activity measurements of mono-radionuclide sources were performed over periods from 200 days up to four decades at 14 laboratories across the globe. Residuals from the exponential nuclear decay curves were inspected for annual oscillations. Systematic deviations from a purely exponential decay curve differ from one data set to another and are attributable to instabilities in the instrumentation and measurement conditions. The most stable activity measurements of alpha, beta-minus, electron capture, and beta-plus decaying sources set an upper limit of 0.0006% to 0.008% to the amplitude of annual oscillations in the decay rate. Oscillations in phase with Earth's orbital distance to the Sun could not be observed within a to range of precision. There are also no apparent modulations over periods of weeks or months. Consequently, there is no indication of a natural impediment against sub-permille accuracy in half-life determinations, renormalisation of activity to a distant reference date, application of nuclear dating for archaeology, geo- and cosmochronology, nor in establishing the SI unit becquerel and seeking international equivalence of activity standards. © 2016 The Authors. Published by Elsevier B.V.
On decay constants and orbital distance to the Sun—part I: alpha decay
(IOP Publishing, 2016-11-28) Pommé, S; Stroh, H; Paepen, J; Van Ammel, R; Marouli, M; Altzitzoglou, A; Hult, M; Kossert, K; Nähle, O; Schrader, H; Juget, F; Bailat, C; Nedjadi, Y; Bochud, F; Buchillier, T; Michotte, M; Courte, S; van Rooy, MW; van Staden, MJ; Lubbe, L; Simpson, BRS; Fazio, A; De Felice, D; Jackson, TW; van Wyngaardt, WM; Reinhard, MI; Golya, J; Bourke, S; Roy, T; Galea, R; Keightley, JD; Ferreira, KM; Collins, SM; Ceccatelli, A; Verheyen, L; Bruggeman, M; Vodenik, M; Korun, M; Chisté, V; Amiot, MN
Claims that proximity to the Sun causes variation of decay constants at permille level have been investigated for alpha decaying nuclides. Repeated decay rate measurements of 209Po, 226Ra, 228Th, 230U, and 241Am sources were performed over periods of 200 d up to two decades at various nuclear metrology institutes around the globe. Residuals from the exponential decay curves were inspected for annual oscillations. Systematic deviations from a purely exponential decay curve differ in amplitude and phase from one data set to another and appear attributable to instabilities in the instrumentation and measurement conditions. The most stable activity measurements of α decaying sources set an upper limit between 0.0006% and 0.006% to the amplitude of annual oscillations in the decay rate. There are no apparent indications for systematic oscillations at a level of weeks or months. Oscillations in phase with Earth's orbital distance to the sun could not be observed within 10−5–10−6 range precision. © The Authors CC BY 3.0 licence
On decay constants and orbital distance to the Sun—part II: beta minus decay
(IOP Publishing, 2016-11-28) Pommé, S; Stroh, H; Paepen, J; Van Ammel, R; Marouli, M; Altzitzoglou, A; Hult, M; Kossert, K; Nähle, O; Schrader, H; Juget, F; Bailat, C; Nedjadi, Y; Bochud, F; Buchillier, T; Michotte, M; Courte, S; van Rooy, MW; van Staden, MJ; Lubbe, L; Simpson, BRS; Fazio, A; De Felice, D; Jackson, TW; van Wyngaardt, WM; Reinhard, MI; Golya, J; Bourke, S; Roy, T; Galea, R; Keightley, JD; Ferreira, KM; Collins, SM; Ceccatelli, A; Verheyen, L; Bruggeman, M; Vodenik, M; Korun, M; Chisté, V; Amiot, MN
Claims that proximity to the Sun causes variations of decay constants at the permille level have been investigated for beta-minus decaying nuclides. Repeated activity measurements of 3H, 14C, 60Co, 85Kr, 90Sr, 124Sb, 134Cs, 137Cs, and 154Eu sources were performed over periods of 259 d up to 5 decades at various nuclear metrology institutes. Residuals from the exponential decay curves were inspected for annual oscillations. Systematic deviations from a purely exponential decay curve differ in amplitude and phase from one data set to another and appear attributable to instabilities in the instrumentation and measurement conditions. Oscillations in phase with Earth's orbital distance to the Sun could not be observed within 10−4–10−5 range precision. The most stable activity measurements of β− decaying sources set an upper limit of 0.003%–0.007% to the amplitude of annual oscillations in the decay rate. There are no apparent indications for systematic oscillations at a level of weeks or months. © The Authors CC BY 3.0 licence
On decay constants and orbital distance to the Sun—part III: beta plus and electron capture decay
(IOP Publishing, 2016-11-28) Pommé, S; Stroh, H; Paepen, J; Van Ammel, R; Marouli, M; Altzitzoglou, T; Hult, M; Kossert, K; Nähle, O; Schrader, H; Juget, F; Bailat, C; Nedjadi, Y; Bochud, F; Buchillier, T; Michotte, C; Courte, S; van Rooy, MW; van Staden, MJ; Lubbe, J; Simpson, BRS; Fazio, A; De Felice, P; Jackson, TW; van Wyngaardt, WM; Reinhard, MI; Golya, J; Bourke, S; Roy, T; Galea, R; Keightley, JD; Ferreira, KM; Collins, SM; Ceccatelli, A; Verheyen, L; Bruggeman, M; Vodenik, B; Korun, M; Chisté, V; Amiot, MN
The hypothesis that seasonal changes in proximity to the Sun cause variation of decay constants at permille level has been tested for radionuclides disintegrating through electron capture and beta plus decay. Activity measurements of 22Na, 54Mn, 55Fe, 57Co, 65Zn, 82+85Sr, 90Sr, 109Cd, 124Sb, 133Ba, 152Eu, and 207Bi sources were repeated over periods from 200 d up to more than four decades at 14 laboratories across the globe. Residuals from the exponential nuclear decay curves were inspected for annual oscillations. Systematic deviations from a purely exponential decay curve differ from one data set to another and appear attributable to instabilities in the instrumentation and measurement conditions. Oscillations in phase with Earth's orbital distance to the sun could not be observed within 10−4–10−5 range precision. The most stable activity measurements of β+ and EC decaying sources set an upper limit of 0.006% or less to the amplitude of annual oscillations in the decay rate. There are no apparent indications for systematic oscillations at a level of weeks or months. © The Authors CC BY 3.0 licence
Preparation of certified reference materials for gross alpha beta measurement
(South Pacific Environmental Radioactivity Association, 2018-11-06) Wilsher, KL; Harrison, JJ; van Wyngaardt, WM; Lee, S; Mokhber-Shahin, L
Gross alpha beta measurement techniques are used for rapid radioanalytical screening of both solid and liquid samples for environmental, scientific and industrial purposes. A number of gross alpha beta measurement techniques are available depending on the sample matrix and each should report the gross or total alpha or beta radioactivity relative to the alpha or beta emitting radionuclide in the calibration source. To establish measurement accuracy and reliability, certified reference materials (CRMs) which are traceable to a national standard should be used to prepare a calibration source in the same geometry as the sample. it was our aim to develop solid CRMs for gross alpha beta techniques using a quartz mineral spiked with standardised and traceable radiotracer solutions. The quartz mineral was pulverised and then sieved to prepare a starting material which had a narrow particle size distribution range to reduce the likelihood of size fractionation. A standard operating procedure for the Malvern Mastersizer 2000 was developed to assess the adequacy of the starting material with the effect of ultrasonics and pump speed being investigated. The starting material vi/as spiked with either 241Am or spiking 99Sr/90Y to prepare the alpha CRM or beta CRM respectively. The solutions were standardised by ANSTO Radionuclide Metrology to provide direct traceability to the Austral an National Standard tor Radioactivity. Spiking was performed using the acetone bath method. The sieved quartz material was mixed with acetone in a large round-bottom flask and accurately known quantities of radionuclide solution added. The flask was rotated on a rotary evaporator tor a few hours to ensure an even distribution of the radionuclide through the quartz. The acetone was evaporated, the dry spiked quartz material transferred to a poly-ethylene bottle and further homogenised by shaking for a few hours using a Turbula mixer. Homogeneity testing using 10 aliquots from each CRM and radionuclide losses on the rotary evaporator glassware and mixing vessel were established using radiochemical separation and alpha spectrometry tor 24‘Am and Liquid Scintillation Counting (LSC) for 90Sr/90Y. Each sample for testing underwent a separation and purification process that included dissolution, precipitation and re-dissolution and column purification using Eichrom® pre-packed cartridge stack of TEVA®, TRU® and Sr-Spec® resins. Canberra Alpha Analyst and Apex Alpha Counting Software was used tor Alpha spectrometry and 90Sr/90Y was measured on a Packard Tri Carb 3lOOTR LSC. This CRM is intended to be used in gross alpha beta counting instrumentation such as gas flow proportional counters and plastic scintillator detector chambers in accordance with lSO18589-6 Measurement of radioactivity in the environment — Soil Part 6: Measurement of gross alpha and gross beta activities and ultimately to be available tor commercial use.
Primary standardisation of technetium-99m by liquid scintillation coincidence counting
(Elsevier B. V., 2020-02) van Wyngaardt, WM; Tobin, SM; Lee, S; Smith, ML; Jackson, TW; Ilter, J; Howe, B; Sarbutt, A
Technetium-99m was standardised by the 4π(LS)ce-γ coincidence extrapolation method. Sensitivity of the 4π(LS) channel to two types of radiation, namely conversion electrons and γ-rays, resulted in incorrect activity values being obtained when this was not adequately accounted for. Measurements were more robust when the LS detection efficiency was optimised, and when a γ-window setting was used that monitored the combined LS efficiency for conversion electrons and γ-rays. The primary standard was internationally compared through participation in the BIPM.RI(II)-K4.Tc99m key comparison. © 2019 Elsevier Ltd
Results of an international comparison of activity measurements of 68Ge
(Elsevier B. V., 2018-04) Cessna, JT; Fitzgerald, R; Zimmerman, BE; Laureano-Pérez, L; Bergeron, DE; van Wyngaardt, WM; Smith, ML; Jackson, TW; Howe, B; da Silva, CJ; Iwahara, A; da Cruz, PAL; Zhang, M; Liu, H; Liang, JC; Fréchou, C; Bobin, C; Cassette, P; Kossert, K; Nähle, O; Marganiec-Gałązka, J; Joseph, L; Ravindra, A; Kulkarni, DN; Yunoki, A; Sato, Y; Lee, KB; Lee, JM; Agusbudiman, A; Dziel, T; Listkowska, A; Tymiński, Z; Sahagia, M; Antohe, A; Ioan, MR; Luca, A; Krivosek, M; Ometakova, J; Javornik, A; Zalesakova, M; García-Toraño Martinez, E; Roteta, M; Mejuto, M; Nedjadi, Y; Juget, F; Yuan, MC; Yeh, CY; Yeltepe, E; Dirican, A; Keightley, JD; Pearce, AK
An international key comparison, identifier CCRI(II)-K2.Ge-68, has been performed. The National Institute of Standards and Technology (NIST) served as the pilot laboratory, distributing aliquots of a 68Ge/68Ga solution. Results for the activity concentration, CA, of 68Ge at a reference date of 12h00 UTC 14 November 2014 were submitted by 17 laboratories, encompassing many variants of coincidence methods and liquid-scintillation counting methods. The first use of 4π(Cherenkov)β-γ coincidence and anticoincidence methods in an international comparison is reported. One participant reported results by secondary methods only. Two results, both utilizing pure liquid-scintillation methods, were identified as outliers. Evaluation using the Power-Moderated Mean method results in a proposed Comparison Reference Value (CRV) of 621.7(11) kBq g−1, based on 14 results. The degrees of equivalence and their associated uncertainties are evaluated for each participant. Several participants submitted 3.6 mL ampoules to the BIPM to link the comparison to the International Reference System (SIR) which may lead to the evaluation of a Key Comparison Reference Value and associated degrees of equivalence. An international key comparison, identifier CCRI(II)-K2.Ge-68, has been performed. The National Institute of Standards and Technology (NIST) served as the pilot laboratory, distributing aliquots of a 68Ge/68Ga solution. Results for the activity concentration, CA, of 68Ge at a reference date of 12h00 UTC 14 November 2014 were submitted by 17 laboratories, encompassing many variants of coincidence methods and liquid-scintillation counting methods. The first use of 4π(Cherenkov)β-γ coincidence and anticoincidence methods in an international comparison is reported. One participant reported results by secondary methods only. Two results, both utilizing pure liquid-scintillation methods, were identified as outliers. Evaluation using the Power-Moderated Mean method results in a proposed Comparison Reference Value (CRV) of 621.7(11) kBq g−1, based on 14 results. The degrees of equivalence and their associated uncertainties are evaluated for each participant. Several participants submitted 3.6 mL ampoules to the BIPM to link the comparison to the International Reference System (SIR) which may lead to the evaluation of a Key Comparison Reference Value and associated degrees of equivalence. An international key comparison, identifier CCRI(II)-K2.Ge-68, has been performed. The National Institute of Standards and Technology (NIST) served as the pilot laboratory, distributing aliquots of a 68Ge/68Ga solution. Results for the activity concentration, CA, of 68Ge at a reference date of 12h00 UTC 14 November 2014 were submitted by 17 laboratories, encompassing many variants of coincidence methods and liquid-scintillation counting methods. The first use of 4π(Cherenkov)β-γ coincidence and anticoincidence methods in an international comparison is reported. One participant reported results by secondary methods only. Two results, both utilizing pure liquid-scintillation methods, were identified as outliers. Evaluation using the Power-Moderated Mean method results in a proposed Comparison Reference Value (CRV) of 621.7(11) kBq g−1, based on 14 results. The degrees of equivalence and their associated uncertainties are evaluated for each participant. Several participants submitted 3.6 mL ampoules to the BIPM to link the comparison to the International Reference System (SIR) which may lead to the evaluation of a Key Comparison Reference Value and associated degrees of equivalence. © 2021 Elsevier Ltd.
Results of the CCRI(II)-S12.H-3 supplementary comparison: comparison of methods for the calculation of the activity and standard uncertainty of a tritiated-water source measured using the LSC-TDCR method
(Elsevier B. V., 2018-04) Cassette, P; Altzitzoglou, T; Anthohe, A; Rossi, M; Arinc, A; Capogni, M; Galea, R; Gudelis, A; Kossert, K; Lee, KB; Liang, J; Nedjadi, Y; Oropesa Verdecia, P; Shilnikova, T; van Wyngaardt, WM; Ziemek, T; Zimmerman, BE
A comparison of calculations of the activity of a 3H2O liquid scintillation source using the same experimental data set collected at the LNE-LNHB with a triple-to-double coincidence ratio (TDCR) counter was completed. A total of 17 laboratories calculated the activity and standard uncertainty of the LS source using the files with experimental data provided by the LNE-LNHB. The results as well as relevant information on the computation techniques are presented and analysed in this paper. All results are compatible, even if there is a significant dispersion between the reported uncertainties. An output of this comparison is the estimation of the dispersion of TDCR measurement results when measurement conditions are well defined. © 2017 Elsevier Ltd.

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