Design and implementation of a differential scanning calorimeter for the simultaneous measurement of small angle neutron scattering

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dc.contributor.authorPullen, SAen_AU
dc.contributor.authorBooth, Nen_AU
dc.contributor.authorOlsen, SRen_AU
dc.contributor.authorDay, Ben_AU
dc.contributor.authorFranceschini, Fen_AU
dc.contributor.authorMannicke, Fen_AU
dc.contributor.authorGilbert, EPen_AU
dc.date.accessioned2017-04-27T05:34:02Zen_AU
dc.date.available2017-04-27T05:34:02Zen_AU
dc.date.issued2014-04-08en_AU
dc.date.statistics2016-10-10en_AU
dc.description.abstractFor almost 30 years, at synchrotron facilities, it has been possible to perform small-angle x-ray scattering experiments whilst simultaneously measuring differential scanning calorimetry (DSC). However, a range of challenges exist to enable the collection of simultaneous small-angle neutron scattering (SANS) and DSC data associated not only with intrinsic flux limitations but also scattering geometry and thermal control. The development of a DSC (temperature range ca. −150 ◦C to 500 ◦C) suitable for SANS is detailed here and its successful use is illustrated with combined measurements on a binary blend of normal alkanes in which one component has been deuterium labelled. © 2014, IOP Publishing Ltden_AU
dc.identifier.articlenumber055606en_AU
dc.identifier.citationPullen, S. A., Booth, N., Olsen, S. R., Day, B., Franceschini, F., Mannicke, F. & Gilbert, E. P. (2014). Design and implementation of a differential scanning calorimeter for the simultaneous measurement of small angle neutron scattering. Measurement Science and Technology, 25(5), 055606. doi:10.1088/0957-0233/25/5/055606en_AU
dc.identifier.govdoc7359en_AU
dc.identifier.issn0957-0233en_AU
dc.identifier.issue5en_AU
dc.identifier.journaltitleMeasurement Science and Technologyen_AU
dc.identifier.urihttp://dx.doi.org/10.1088/0957-0233/25/5/055606en_AU
dc.identifier.urihttp://apo.ansto.gov.au/dspace/handle/10238/8636en_AU
dc.identifier.volume25en_AU
dc.language.isoenen_AU
dc.publisherIOP Scienceen_AU
dc.subjectNeutronsen_AU
dc.subjectCalorimetryen_AU
dc.subjectX-ray diffractionen_AU
dc.subjectDataen_AU
dc.subjectDeuteriumen_AU
dc.subjectTemperature rangeen_AU
dc.titleDesign and implementation of a differential scanning calorimeter for the simultaneous measurement of small angle neutron scatteringen_AU
dc.typeJournal Articleen_AU
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