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Please use this identifier to cite or link to this item: http://apo.ansto.gov.au/dspace/handle/10238/7797

Title: Design and implementation of a differential scanning calorimeter for the simultaneous measurement of small angle neutron scattering
Authors: Pullen, SA
Booth, N
Olsen, SR
Day, B
Franceschini, F
Mannicke, D
Gilbert, EP
Keywords: SYNCHROTRONS
X-RAY DETECTION
GEOMETRY
ALKANES
DEUTERIUM
DATA
Issue Date: 8-Apr-2014
Publisher: IOP Science
Citation: Pullen, S. A., Booth, N., Olsen, S. R., Day, B., Franceschini, F., Mannicke, F. ... Gilbert, E. P. (2014). Design and implementation of a differential scanning calorimeter for the simultaneous measurement of small angle neutron scattering. Measurement Science and Technology, 25(5), 055606. doi: http://dx.doi.org/10.1088/0957-0233/25/5/055606
Abstract: For almost 30 years, at synchrotron facilities, it has been possible to perform small-angle x-ray scattering experiments whilst simultaneously measuring differential scanning calorimetry (DSC). However, a range of challenges exist to enable the collection of simultaneous small-angle neutron scattering (SANS) and DSC data associated not only with intrinsic flux limitations but also scattering geometry and thermal control. The development of a DSC (temperature range ca. −150 °C to 500 °C) suitable for SANS is detailed here and its successful use is illustrated with combined measurements on a binary blend of normal alkanes in which one component has been deuterium labelled.
URI: http://dx.doi.org/10.1088/0957-0233/25/5/055606
http://apo.ansto.gov.au/dspace/handle/10238/7797
ISSN: 1757-899X
Appears in Collections:Journal Articles

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