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|Title: ||Design and implementation of a differential scanning calorimeter for the simultaneous measurement of small angle neutron scattering|
|Authors: ||Pullen, SA|
|Issue Date: ||8-Apr-2014|
|Publisher: ||IOP Science|
|Citation: ||Pullen, S. A., Booth, N., Olsen, S. R., Day, B., Franceschini, F., Mannicke, F. ... Gilbert, E. P. (2014). Design and implementation of a differential scanning calorimeter for the simultaneous measurement of small angle neutron scattering. Measurement Science and Technology, 25(5), 055606. doi: http://dx.doi.org/10.1088/0957-0233/25/5/055606|
|Abstract: ||For almost 30 years, at synchrotron facilities, it has been possible to perform small-angle x-ray scattering experiments whilst simultaneously measuring differential scanning calorimetry (DSC). However, a range of challenges exist to enable the collection of simultaneous small-angle neutron scattering (SANS) and DSC data associated not only with intrinsic flux limitations but also scattering geometry and thermal control. The development of a DSC (temperature range ca. −150 °C to 500 °C) suitable for SANS is detailed here and its successful use is illustrated with combined measurements on a binary blend of normal alkanes in which one component has been deuterium labelled.|
|Appears in Collections:||Journal Articles|
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